• 专利附录
  • 专利说明
  • 权利要求
  • 类似技术
  • 同族专利
  • 引用文献
  • 法律状态
  • 优先权
    • 专利摘要:
    The invention relates to chemical weed control agents and allows for an increase in the effectiveness of the herbicidal agent. As an active ingredient, a compound of the formula YN — CH = CH — CH = CH — CH = C — NH — SO 2 —C = NN — CHR 1 = CHR 1 N = C (CH 3 ) —N (CN 3 ) is introduced into the agent -C = X, where X is oxygen or sulfur R 1 is methoxycarbonyl, ethoxycarbonyl, aminocarbonyl or methylsulfonyl YN - 2,6-difluoro, 2,6-dichloro, 2,6-dibrom, 2-fluoro-6-chloro, 2-chloro-6-bromo, 2-chloro-6-methyl, 2-bromo-6- methoxy, 2-difluoromethoxy-6-methyl, 2-methyl-6-nitro, 6-methyl-2-methoxycarbonyl, 2,6-dichloro (bromo) -3-methyl, 2-bromo-6-chloro-3-methyl or 6-fluoro-3-methyl-2-methoxycarbonyl. The tool contains, by weight. %: active ingredient 25 kaolin 60 silicic acid 10 calcium ligninsulfonate 3 Sodium N-methyl-N-oleyl-taurite 2. Compared with the known agent based on triazolpyrimidinesulfonamides, this agent has 1.5-4 times more herbicidal activity. 3 tab.
    公开号:SU1616507A3
    申请号:SU884356000
    申请日:1988-06-30
    公开日:1990-12-23
    发明作者:Крюгер Мартин；Вестерманн Юрген；Арндт Фридрих；Риис Ричард；Джордж Хант Рассел
    申请人:Шеринг Аг (Фирма)；
    IPC主号:
    专利说明:

    2,6-Dichloroanilide 3-methoxycarbonyl 5, 6-dimethyl-7-TIOXO-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazine-2 sulfonic acid
    2,6-Dichloro-3-methylanilide 3-methoxycarbonyl-5, 6-dimethyl-7-oxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2-sulfonic acid
    2,6-Dichloro-3-methylanilide 3-methoxycarbonyl-5, 6-dimethyl-7-thioxo-6,7 dihydropyrazole (1,5-a) - (1,3,5) -triazin-2-sulfonic acid
    2-Chloro-6-fluoroanilide 3-methoxycarbonyl-5, 6-dimethyl-7-oxo-6,7-di304-305
    262-264
    312-314
    240-242
    1616507 About
    Continuation of table 1
    iz: i :::::::::::::::::::::; ::: r :: L ::
    hydro-pyrazole- (1,5-a) - (1,3,5) -tri-azin-2-sulfonic acids
    2-Chloro-6-fluoroanilide 3-methoxycarbo-285-286 nyl-5,6-dimethyl-7-thioxo-6,7-dihydro-piraeol (1,5-a) - (1,3,5) triazine-2-sulfonic acid
    2-Chloro-6-methylanilide 3-methoxycar-259-261 bonyl-5,6-dimethyl-7-oxo-6,7-dihydro-pyrazole- (1,5-a) - (1,3,5 a) -triazine-2-sulfonic acid
    2-Chloro-6-methylanilide 3-methoxycar-295-297 bonyl-5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) triazine-2-sulfonic acid
    2,6-Dibromanalide 3-methoxycarbonyl-293-295 5,6-dimethyl-7-oxo-6, / - dihydro-pyrazole- (1,5-a) - (1,3,5) -triazin-2- sulfonic acids
    2,6-DibromoNILide 3-methoxycarbonyl-327-330 5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazine-2-sulfonic acids
    2-Methyl-6-nitroanilide-hydrate 3-me-230-232 toxycarbonyl-5,6-dimethyl-7-oxo6, 7-dihydropyrazole (1,5-a) - (1,3,5) - triazin-2 -sulfonic acid
    2-Methyl-6-nitroanilide 3-methoxy-271-274 carbonyl-5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazole (1 , 5-a) - (1,3,5) -triazin-2-sulfonic acids
    2-Methoxycarbonyl-6-methylenchide 3-210-212 methoxycarbonyl-5,6-dimethyl-7-thioxo-6, 7-dihydropyrazol- (1,5-a) - (1,3,5) -triazine- 2-sulfonic acid
    2-Bromo-6-methoxyanalide-3-methy-276-277 toxi-carbonyl-5,6-dimethyl-7-thioxo-6, 7-dihydropyrazole (1,5-a) - (1,3,5 ) - triazin-2-sulfonic acid
    2,6-DichlororanALID 3-ethoxycarbonyl-283-284 5,6-dimethyl-7-oxo-6,7-dihydropyrazole- (1,5-a) - (1,3,5) -triazine-2-sulfonic acids
    2,6-Difluoroanilide 3-ethoxycarbonyl-221-223 5,6-dimethyl-7-oxo-6,7-dihydropyrazole (1, 5-a) - (1,3,5) -triazin-2-sulfonic acid
    2-Chloro-6-fluoroanilide 3-ethoxycarbo-214-217 nyl-5,6-dimethyl-7-oxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazine - 7-sulfonic acid
    2,6-Dichloro-3-methylanilide 3-ethoxy-228-230 carbonip-5 6-dimethyl-7-oxo-6,7-di: L L ..... z ::: i :: z: z
    hydropiraeol (1,5-a) - (1,3,5) -trie zin-2-sulfonic acids
    212,6-7 bromanilide 3-ethoxycarbonyl-295-297 5,6-dimethyl-7-oxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2- sulfonic acids
    222-Bromo-6-chloroanilide 3-ethoxycarbo-285-286 nyl-5,6-dimethyl-7-oxo-6,7-dihydro-pyrazole (1,5-a) - (1,3,5) triazine-2-sulfonic acid
    232,6-Liftoanilide 3-ethoxycarbonyl 272-274 5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2-sulfonic acid
    242,6-Dichloro-3-methylanilide 3-ethoxy-257-259 carbonyl-5,6-dimethyl-7-thioxo-6,7 dihydropyrazole (1,5-a) - (1,3,5) -triazine -2 sulfox slots
    252-Chloro-6-fluoro-NILide 3-toxycarbo-232-235 nyl-5,6-dimethyl-7-thioxo-6,7-dihydro-pyrazole (1,5-a) - (1,3,5) -triazine-2-sulfonic acid
    262,6-Difluoroanilide 3-ethoxycarbonyl-214-216 5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2-sulfonic acid
    72-Chloro-6-methylanilide 3-ethoxycarbonyl-5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazine- 2-solvents
    82,6-Dibromanilide 3-ethoxycarbonyl-285-287 5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2-sulfonic acid
    92-Bromo-6-chloroanilide 3-ethoxycarbo-291-293 nyl-5,6-dimethyl-7-thioxo-6,7-dihydro-pyrazole (1,5-a) - (1,3,5) -triazine-2-acidic acids
    02,6-Dichloroanlide 3-aminocarbonyl-303-305 5,6-dimethyl-7-oxo-6,7-dihydropyrazole C1, 5-a) - (1,3,5) -triazin-2-sulfonic acid
    2,6-Dichloroanilide-3-aminocarbonsh-225-296
    5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2-sulfonic acid slots
    22,6-Dichloroanilide 3-methylsulfonyl-289-292 5,6-dimethyl-7-oxo-6,7-dihydro-pyrazol (1,) - (1,3,5) -triazin-2-sulfonic acid
    32,6-Dichloro-3-methylanilide 3-methyl-273-275 sulphdyl-5,6-dimethyl-7-oxo-6,7-dihydropyrazole (1,5-a) - (1, 3, 5) triazin-2-sulfonic acid
     316165071
    Continuation of table 1
    :: E ::; :: Z ::::::::::::::::::::: I ::: I:
    2,6-DichloroNILide 3-methylsulfonyl-318-320 5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2-sulfonic acid
    2,6-Dichloro-3-methylanilide 3-methyl-290-293 sul y}) onyl-5,6-dimethyl-7-thioxo-6, 7-dihydropyrazole (1,5-a) - (1, 3,5) - triazin-2-sulfonic acid
    2-Bromo-6-hl6ranid 3-methoxycar-293-294 bonyl-5,6-dimethyl-7-oxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) - triazine -2-sulfonic acid)
    2-Bromo-6-chloro-3-methylanilide 3-me-286-288 tocarbonyl-5,6-dimethyl-7-oxo-6,7-dihydropyrazole (1 ,, 5-a) - (1, 3.5 a) triazin-2-eulfonate
    2,6-Dibromo-3-metsh1anilid 3-labels-205 scicarbonyl-5.6-dimethyl-7-oxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2 sulfonic acid
    2-Difluoromethoxy-6-methylanilide 3-me-198-199 toxicarbonyl-5,6-dimethyl-7-oxo6, 7-dihydropyrazole (1,5-a) - (1,3,5) - triazin-2 α-sulfonic acid
    6-Fluoro-2-methokeicarbonyl-3-methyl-194-195 anilide-3-methoxycarbonyl-5,6-dimethyl-7-ocean-6,7-dihydropyrazole
    (1,5-a) - (1,3,5) -triazin-2-sulfonic acid
    2-Bromo-6-Chloranilide 3-methoxycar-206 bonyl-5,6-dimethyl-7-thiokeo-6,7-dihydropyrazolS1,5-a) - (1,3,5) - triazin-2-sulfonic acid
    2-Bromo-6-chloro-3-methylanilide 3-me-307-309 toxycarbonyl-5,6-dimethyl-7-thiokeo-6, 7-dihydropyrazole (1.5, -a) - (1, 3.5 triazin-2-sulfonic acid
    2-Difluoromethoxy-6-methylanilide 3- 36-238 methokecarbonyl-5,6-dimetsh1-7thioxo-6, 7-dihydropyrazole (1,5-a) - (1,3,5) -triazine -.- eulfonic acid
    6-Fluoro-2-methoxycarbonyl-3-methyl-264-265 anilide-3-methoxycarbonyl-5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1 , 3,5) -triazin-2-sulfonic acid
    2-Metsh1-6-nitroanilide 3-etkei-162 carbonyl-5,6-dimethyl-7-thiokeo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazine -2-eulfonic acid
    2-Chloro-6-methylanilide 3-ethoxycar-240
    Bonil-5,6-dimethyl-7-ox0-6,7-dihyd 161650716 Continuation of table 1
    zzzzz :: iz: z ::: i ::: i:
    ro-pyra9al (1,5-a) -triaein-2-sulfonic acids
    472-Methyl-6-nitroanilide 3-ethoxycar-235-236
    bonyl-5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazine-2-sulfonic acids
    17
    1616507
    18
    Continuation of table 2
    Compound
    Plant damage assessment
    Tg I No Bg I Not I St I Ab Tma | Vi Tch | So 1 Her 1 Se | Ga
    Compound A
    , N-N SIS-VV NHSOr
    Compound
    Plant damage assessment
    Tg
    .r J-
    J But j Вг 1 Ly I Me I, Not St TAI I Ma 1 Vi 1 Ch

    0 1
    0 1
    0 0 0 0 0 0
    0 0 0 2 0 0 0 2 0 0
    3 3 3 4 2 3 3 3 2 2
    4 3 3 4 3 3 3 3 2 3
    3 3 4 3 3 3 3 3 2 2
    4 3 3 2 4 3 2
    Table3
    St TAI I Ma 1 Vi 1 Ch
    4 4 3 4 2 3 2 4 3 3
    2 2 2 2 2 2 3 3 1 2
    3 3 2 3 3 4 2 3 2 2
    2 3 3 1 3 2 2 2 1 2
    3 3 2 4 4 4 2 4 2 3
    Ga
    4 3 3 4 3 3 3 3 3 3
    权利要求:
    Claims (4)
    [1]
    12
    14
    ten
    1 13 2 3 0 3 3 2
    Compound
    BUT
    Table3
    Compound
    Plant damage assessment
    Tg
    But} г у ΐ ΐ Me, Not 56 ^ AB Ma ν ί СЬ
    (1,5-a) - (1,3,5) -triazin-2-sulfonic acids
    [2]
    2 3
    four
    3
    3
    four
    3
    four
    3
    2 · 2 2 4
    2 4
    2 3
    2 4
    2 3 2 3 2 2 2 3 2 3
    2 3
    2 2
    2 1
    2 2
    0 00000 0 00
    2 2
    0 4
    2 3
    2 '3 3
    0 4 1
    2 3 2
    2-Chloro-6-methylanilide 3-ethoxycarbonyl-5, 6-dimethyl-7-oxo-6,7-dihyd318-320
    290-293
    293-294
    286-288
    205
    198-199
    194-195
    206
    307-309
    36 36-238
    264-265
    162
    46
    240
    15
    1616507
    sixteen
    Continued. Table 1
    ~ Ί Τ "~~ ΤΞ ~
    ro-piraeol (1,5-a) -triaein-2-sulfonic acid
    47 2-Methyl-6-nitroanilide 3-ethoxycar- 235-236
    bonyl-5,6-dimethyl-7-thioxo-6,7 dihydropyrazole (1, 5-a) - (1, 3.5) triazine-2-sulfonic acid
    table 2
    Compound Plant damage assessment Tg But 1 vg| Not I 81I AB 'ί! yo1 — ίeleven νί | smiling I 50 | EC I- | Sa one 0 0 3 3 2 3 onefour four four 3 3 3 3 2 2 2 3 3 2 2 four 3 3 four four 3 3 3 0 0 · 3 3 one 2 four 3 3 3 3 four 2 four one 0 3 3 3 3 four 3 four four 3 four four five 0 0 3 3 3 3 four 3 four 2 2 2 3 6 0 one 2 3 3 2 four four four 3 3 2 four 7 0 one 2 3 2 2 four 3 3 2 2 2 2 eight one 2 3 3 2 2 four 3 four four 3 four 3 9 0 one 2 3 2 2 four 3 3 3 2 3 3 ten one 2 3 3 3 2 four 3 3 3 3 2 3 eleven 0 - four 3 - 3 four four - - - 3 3 12 one - four 3 - 3 four four - - - four 3 13 0 - four 3 - 2 four four - - - 3 four 14 one - four 3 - 2 four 3 - - - 2 four 15 0 - one one - 0 four 0 - - - 0 0 sixteen one - one 2 - 0 four - - - - one 2 17 0 - 3 3 - 3 four - - - - 3 3 18 0 - 3 3 - 3 3 - - - - 2 2 nineteen 0 - 3 3 - 3 four - - - - 2 2 20 0 - 3 2 2 one four - - - - 0 2 21 one - 3 2 - one four - - - - 3 3 22 0 - - - - 3 four - - - - four four 23 0 - 3 3 - 3 four - - - - 3 3 24 0 - 3 3 - 2 four - - - - 2 •four 25 0 - 3 2 - 2 four - - - - 0 2 26 0 - 2 2 - one four - - - - 0 2 27 0 - 2 one - 0 3 - - - - 0 3 28 one - 3 2 - R four - - - - 0 3 29 0 - - - - 3 four - - - - four four thirty 0 - 3 3 - 0 four . - - - - 3 3 31 one - 3 3 - 0 four - - - - 3 3 32 0 - - - - 0 2 - - - - one 2 33 0 - - - - 2 four - - - 2 3 34 0 - - - - 0 3 - - - - 0 2 35 0 - - - - one four - - - - ABOUTfour. four 36 0 - four 3 - 2 four 2 - - - 3 four 37 one - 3 3 - - 3 3 3 - - - aboutί- 3 ' 38 0 - 3 3 - one 3 one - - - 0 2 39 one - 3 3 - 2 3 3 - - - 3 2 40 0 - 3 3 - 2 3 2 - - - one 2
    17
    18
    Continuation of table 2
    1616507
    Compound
    41 2-43
    42 0 - 3 3
    43 1-33
    44 2 - 3 3
    45 0 - 4 3
    46 0 - 3 3
    47 0 - 3 3
    Control
    (unprocessed) 0000 A *
    (known) 0 0 2 2
    Plant damage assessment
    | 5G "I AB ^ Ma R Pb Ro Es Es Ze ^ | Ca
    2-Methyl-6-nitroanilide 3-ethoxycarbonyl-5,6-dimethyl-7-thioxo-b, 7di hydro-pyrazole (1 "5-a) - (1,3,5) -triaine-2-sulfonic
    2-Bromo-6-Chloranilide 3-methoxycarbonyl-5,6-dimethyl-7-thioxo-6.7 dihydropyrazole (1,5-a) - (1,3,5) triazin-2-sulfonic acid 2-Bromo- 6-chloro-3-methylanilide 3-methoxycarbonyl-5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5, -a) (1,3,5) -triazin-2-sulfonic acids 2-Difluoromethoxy -6-methylanilide 3methoxycarbonyl-5,6-dimethyl-7thioxo-6,7-dihydropyrazole (1,5-a) (1,3,5) -triazin-2-sulfonic acid 6-Fluoro-2-methoxycarbonyl-3 -methylanilide -Z-methoxycarbonyl-5, 6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2sulphoki slots
    2-Difluoromethoxy-6-methylanilide 3-methoxycarbonyl-5,6-dimethyl-7-oxo6.7-dihydropyrazole (1,5-a) - (1,3,5) triazin-2-sulfonic acid 6-Fluoro 2-methoxycarbonyl-3-methylanilide-3-methoxycarbonyl-5,6-dimethyl-7-oxo-6,7-dihydropyrazole
    2.6- Dibromo-3-methylanilide 3-methoxycarbonyl-5,6-dimethyl-7-oxo-6,7 dihydropydol sol (1,5-a) - (1,3,5) -triazine-2-sulfonic acids
    2.6- Dichloro-3-methylanilide 3-methylsulphonyl-5,6-dimethyl-7-thioxo; 6.7-dihydropyrazole (1,5-a) - (1,3,5) triazin-2-sulfonic acid 2-Bromo -6-chloroanilide 3-methoxycarbonyl-5,6-dimethyl-7-oxo-6,7-diI
    hydro-pyrazole (1,5-a) - (1,3,5) trizin-2-sulfonic acid 2-Bromo-6-chloro-3-methylanilide 3-me ~ tocarbonyl-5,6-dimethyl-7-oxo6 .7-dihydropyrazole (1,5-a) - (1,3,5) triazin-2-sulfoxpot
    2.6- Dichloroanilide 3-methylsulfonyl; 5.6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2 sulfonic acid
    2.6- 3-methyl-273-275 dichloro-3-methylanilide
    sulfonyl-5,6-dimethyl-7-oxo6.7-dihydropyrazole (1,5-a) (1,3,5) -tri-aein-2-sulfonic acids
    13
    16.6507
    14
    one
    34
    35
    36
    37
    38
    39
    40
    ::
    Continued. 3
    41
    42
    43
    44
    45
    2.6- 3-methylsulphonyl dihydroranilide 289-292
    5.6-dimethyl-7-oxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2 sulfonic acid
    2.6- Dichloroanilide-3-aminocarboiyl- 295-296
    5.6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triaein-2 sulfonic acid
    2.6- 3-aminocarbonyl dihporanilide- 303-305
    5.6-dimethyl-7-oxo-6,7-dihydropyrene sol (1,5-a) - (1,3,5) -triaen-2 sulfonic acid
    2-Bromo-6-chloroanilide 3-ethoxycarbo-291-293 nyl-5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazine2 sulfonic acid
    2.6- Dibromanilide 3-ethoxycarbonyl- 285-287
    5.6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2 sulfonic acid
    2-Chloro-6-methylanilide 3-ethoxycarbonyl-5,6-dimethyl-7-thioxo-6,7-dihydro-pyrazole (1,5-a) - (1,3,5) -triazine-2 sulfonic acid
    2.6- Difluoroanilide 3-ethoxycarbonyl- 214-216
    5.6-dimethyl-7-thioxo-6,7-dihydropiraeol (1,5-a) - (1,3,5) -triaein-2 sulfonic acid
    2-Chloro-6-fluoroanilide 3-ethoxycarbo-232-235
    nyl-5,6-dimethyl-7-thioxo-b, 7-dihydr o-pyr zol (1,5-a) - (1,3,5) - triazine-2-sulfonic acids
    2.6- Dichloro-3-methylanilide 3-ethoxy- 257-259
    carbonyl-5,6-dimethyl-7-thioxo-6,7 dihydropyrazole (1,5-a) - (1,3,5) -triazin-2-sulfonic acids
    2.6- Difluoroanilide 3-ethoxycarbonyl ~ 272-274
    5.6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2 sulfonic acid
    2-Bromo-6-chloroanilide 3-ethoxycarbo-285-286 nyl-5,6-dimethyl - / - oco-6,7-dihydropyrazole (1.5 — a) - (1,3,5) -triazine2 sulfonic acid
    2.6- Dibromanilide 3-ethoxycarbonyl- 295-297
    5.6-dimethyl-7-oxo-6,7-dihydropyrazole (1, 5-a) - (1,3,5) -triazin-2 sulfonic acid
    2-methyl-6-nitro, 2-methyl 6-methoxycarbonyl, 2,6 dichloro (bromo) -3-methyl, 2 bromo-6-chloro-3-methyl, 6-fluoro 3-methyl-2-methoxycarbonyl,
    as clay - kaolin, as a salt of ligninsulfonic acid - calcium ligninsulfonate, in the following ratio of components, wt.X:
    Indicated active ingredient 25
    Kaolin 60
    Flint
    acid 10
    Calcium ligninsulfonate 3
    S-methyl-M-oleyl-taurite sodium 2
    Table 1
    Compound Connection name Temperaturemelting, ° C one 2 3 four 2.6-Dichloroanilide 3-methoxycarbonyl; 5.6-dimethyl-7-thioxo-b; 7-dihydropyrazole (1,5-a) - (1,3,5) -triazine-2 sulfonic acid 304-305 five 2,6-Dichl op-3-methyl anilide 3-methoxycarbonyl-5,6-dimethyl-7-oxo-b, 7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2- sulfonic acids 262-264 6 2,6-Dichloro-3-methylanilide 3-methoxycarbonyl-5,6-dimethyl-7-thioxo-6,7 dihydropyrazole (1,5-a) - (1,3,5) -triazin-2-sulfonic acids 312-314 7 2-Chloro-6-fluoroanilide 3-methoxycarbonyl-5,6-dimethyl-7-oxo-b, 7-di- 240-242
    9
    1616507
    ten
    Continued, table. one
    ΞΠΞΣΖ’ΣΣΣ’Ξ’ΣΣΣΖΣΕ
    hydro-pyrazole- (1,5-a) - (1,3,5) -triazin-2-sulfonic acid
    8 2-Chloro-6-fluoroanilide 3-methoxycarbo-285-286 nyl-5,6-dimethyl-7-thioxo-6,7-dihydro-piraeol (1,5-a) - (1,3,5) - triazin2-sulfonic acid
    9 2-Chloro-6-methylanilide 3-methoxycar-259-261 bonyl-5,6-dimethyl-7-oxo-6,7-dihydropyrazole- (1,5-a) - (1,3,5) triazin2-sulfonic acid
    10 2-Chloro-6-methylanilide 3-methoxycar-295-297 bonyl-5,6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) - triazin2-sulfonic acid
    11 2,6-Dibromanalide 3-methoxycarbonyl- 293-295
    5.6-dimethyl-7-oxo-6, / - dihydro-pyrol sol- (1, 5-a) - (1,3,5) -triazine-2 sulfonic acid
    12 2,6-Dibromanilide 3-methoxycarbonyl- 327-330
    5.6-dimethyl-7-thioxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) -triazin-2 • sulfonic acid
    13 2-Methyl-6-nitroanilide hydrate 3-me-230-232
    toxycarbonyl-5,6-dimethyl-7-oxo6.7-dihydropyrazole (1,5-a) - (1,3,5) triazin-2-sulfonic acid
    14 2-Methyl-6-nitroanilide 3-methoxy. - 271-274
    carbonyl-5,6-dimethyl-7-thioxo-6,7 dihydropyrazole (1,5-a) - (1,3,5) -triazole (1.5 — a) - (1,3,5) -triazine- 2-sulfonic acid
    15 2-Methoxycarbonyl-6-methylanilide 3- 210-212
    methoxycarbonyl-5,6-dimethyl-7-thioxo-6,7-dihydro-pyrazole- (1,5-a) (1,3,5) -triazin-2-sulfonic acid
    16 2-Bromo-6-methoxyanalide-3-hydroxy-276-277 toxi-carbonyl-5,6-dimethyl-7-thioxo-6,7-dihydro-piraole (1,5-a) - (1,3, 5) triazin-2-sulfonic acid
    17 2,6-Dichloranalide 3-ethoxycarbonyl- 283-284
    5.6-dimethyl-7-oxo-6,7-dihydropyrazole- (1,5-a) - (1,3,5) -triazin2-sulfonic acid
    18 2,6-Difluoroanilide 3-ethoxycarbonyl- 221-223
    5.6-dimethyl-7-oxo-6,7-dihydropyrazole (1, 5-a) - (1,3,5) -triazin-2 sulfonic acid
    19 2-Chloro-6-fluoroanilide 3-ethoxycarbo-214-217 nyl-5,6-dimethyl-7-oxo-6,7-dihydropyrazole (1,5-a) - (1,3,5) - triazine 7-sulfonic acid
    20 2,6-Dichloro-3-methylanilide 3-ethoxy-228-230 carbonyl-5,6-dimethyl-7-oxo-6,7-di ! 1616507 ιζ
    Continued. Table “1”
    hydropiraeol (1,5-a) - (1,3,5) -treezin2-sulfoxylic acid
    2,6-dibromo, 2-fluoro-6-chloro, 2-chloro-6-bromo, 2-chloro-6-methyl, 2-bromo-6-methoxy, 2-difluoromethoxy-6-methyl,
    [3]
    3 4
    3 2
    3 3
    3 2 3 3 1 2 2 2
    3 3
    3 4
    3 2
    3 2
    4 3
    3 3
    4 4
    3 4
    3 4
    3 2
    3 3
    3 3
    3 3
    4 3
    3 4
    4 3
    3 3
    thirty
    4 1
    50
    6 0
    7 o
    8 o
    9 o
    10 o
    O 3 O 3 O 3 2 4 O 2 O 3 O 3 2 3 O 2 O 2
    4 3
    3 3
    3 3
    3 4
    3 3 3
    3 3 3
    3 3 3
    3 4 3
    [4]
    4 3 3
    Control (unprocessed) 0 A
    (known) 0
    one
    <1
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